Título:
|
Indium Zinc Oxide pyramids with pinholes and nanopipes
|
Autores:
|
Bartolomé Vílchez, Javier ;
Maestre Varea, David ;
Amati, Mateo ;
Cremades Rodríguez, Ana Isabel ;
Piqueras de Noriega, Javier
|
Tipo de documento:
|
texto impreso
|
Editorial:
|
Amer Chemical Soc, 2011-04-28
|
Dimensiones:
|
application/pdf
|
Nota general:
|
info:eu-repo/semantics/restrictedAccess
|
Idiomas:
|
|
Palabras clave:
|
Estado = Publicado
,
Materia = Ciencias: Física
,
Tipo = Artículo
|
Resumen:
|
Micropyramids of zinc-doped indium oxide have been grown by thermal treatments of compacted InN and ZnO powders at temperatures between 700:and 900 degrees C Under argon flow. X-ray diffraction (XRD) measurements and energy-dispersive X-ray (EDS) mappings as well as local EDS spectra enable the identification of rough surfaces of the pyramids with the nucleation of a shell of nanocrystallites with high Zn/In ratio because of the formation of Zn(k)In(2)O(k+3). Some of the pyramids have a truncated tip with pinholes with regular crystalline facets. The apexes of these pinhole's present a hollow core or nanopipe The possible relation of the nanopipes with a dislocation driven growth is discussed. A growth model is proposed from the morphology evolution of the pyramids during the formation of the In(2)O(3)-ZnO (IZO) compound X-ray photoelectron spectroscopy and microscopy (XPS-ESCA) Measurements are used to discuss the Zn incorporation as a dopant and the formation of Zn(k)In(2)O(k+3) ternaries. Cathodoluminescence (CL) in the scanning electron microscopy (SEM) shows a dependence of the luminescence of the microstructures on the Zn concentration and the growth temperature.
|
En línea:
|
https://eprints.ucm.es/id/eprint/23007/1/CremadesAna03.pdf
|